Dimethylmalonic Acid CAS 595-46-0
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2018-09-28 03:33
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Product details
Product Description
Chemical Name | Dimethylmalonic acid CAS 595-46-0 |
Synonyms |
Dimethyl propanedioic acid; |
CAS No. |
595-46-0 |
EINECS No. |
209-867-1 |
Molecular Fomula |
C5H8O4 |
Molecular Weight |
132.11 |
InChI Key |
OREAFAJWWJHCOT-UHFFFAOYSA-N |
Appearance |
White crystal powder |
Assay |
98% min |
Description |
Dimethylmalonic acid is a short-chain dicarboxylic acid occasionally found in human serum. |
Preparation method: |
A synthesis method of dimethyl 2,2-dimethylmalonate is characterized by: firstly, using 2,2-dimethyl-1,3-propanediol as starting material, phosphohexanoic acid as catalyst, oxidizing it to crude 2,2-dimethylmalonate with 50% hydrogen peroxide, then recrystallizing it with deionized water to obtain pure 2,2-dimethylmalonate; secondly, using sodium bisulfate hydrate as catalyst, 2,2-dimethylmalonate is obtained. Methylmalonic acid is esterified with methanol, and the water carrier is alkane. After the reaction, the solvent is used. The product 2,2-dimethylmalonic acid dimethyl ester is obtained by washing, drying and vacuum distillation of anhydrous magnesium sulfate. |
Packing |
1kg, 5kg, 10kg and 25kg packing. |
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